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Properties of substance:
sodium cyanoborohydride
Group of substances:
inorganic
Empirical formula (Hill's system for organic substances):
CH
3
BNNa
Structural formula as text:
NaBH3CN
Molar/atomic mass: 62.84
Melting point (°C):
240-243
Solubility (g/100 g of solvent):
benzene
: insoluble [
Ref.
]
diethyl ether
: insoluble [
Ref.
]
diglyme
: 17.6 (25°C) [
Ref.
]
ethanol
: sparingly soluble [
Ref.
]
hexane
: insoluble [
Ref.
]
isopropylamine
: sparingly soluble [
Ref.
]
methanol
: very soluble [
Ref.
]
tetrahydrofuran
: 37.2 (28°C) [
Ref.
]
tetrahydrofuran
: 41 (46°C) [
Ref.
]
water
: 212 (29°C) [
Ref.
]
water
: 181 (52°C) [
Ref.
]
water
: 121 (88°C) [
Ref.
]
Hygroscopic:
yes
Reactions of synthesis:
Yeild 91%. [
Ref.1
]
NaBH
4
+ HCN → NaBH
3
CN + H
2
References:
Synthesis. - 1976. - No. 3. - pp. 135-146 [DOI:
10.1055/s-1975-23685
]
Общая органическая химия. - Т. 6, под ред. Бартона Д. и Оллиса В.Д. - М.: Химия, 1984. - pp. 245-246, 348-352 [Russian]
Репинская И.Б., Шварцберг М.С. Избранные методы синтеза органических соединений. - Новосибирск, 2000. - pp. 119 [Russian]
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© Collected Ruslan Anatolievich Kiper, burewestnik@mail.ru