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Properties of substance:
trichloroacetic acid
Group of substances:
organic
Physical appearance:
colorless rhombic crystals
Empirical formula (Hill's system for organic substances):
C
2
HCl
3
O
2
Structural formula as text:
CCl3COOH
Molar/atomic mass: 163.38
Melting point (°C):
57.5
Boiling point (°C):
197.5
Solubility (g/100 g of solvent):
1,2-dichloroethane
: soluble [
Ref.
]
ammonia liquid
: very easily soluble [
Ref.
]
diethyl ether
: soluble [
Ref.
]
ethanol
: soluble [
Ref.
]
water
: 120 (25°C) [
Ref.
]
Properties of solutions:
48% (wt.), solvent - water
Dynamic viscosity (mPa·s) = 3.076 (20°)
Density (g/cm
3
) = 1.2682 (20°)
Index of refraction = 1.3977 (20°)
Density:
1.6298 (61°C, g/cm
3
)
Reactions:
Yeild 88%. [
Ref.1
]
CCl
3
COOH + CH
3
OCHCl
2
→ CCl
3
COCl + HCOOCH
3
+ HCl
Refractive index (n
D
):
1.4603 (61°C)
Dissociation:
pK
a
(1) = 0.66 (20°C, water)
pK
a
(1) = 11.6 (25°C, acetic acid)
pK
a
(1) = 1.46 (20°C, formamide)
Permittivity (dielectric constant):
4.6 (60°C)
Dipole moment (D):
1.1 (20°C)
Surface tension (mN/m):
27.8 (80.2°C)
Standard molar enthalpy (heat) of formation Δ
f
H
0
(298.15 K, kJ/mol):
-503.3 (s)
Molar enthalpy (heat) of fusion Δ
fus
H (kJ/mol):
5.88
Heat of combustion (kJ/mol):
388.3
References:
CRC Handbook of Chemistry and Physics. - 90ed. - CRC Press, 2010. - pp. 5-21
CRC Handbook of Chemistry and Physics. - CRC Press, 2002
Seidell A. Solubilities of organic compounds. - 3ed., vol.2. - New York: D. Van Nostrand Company, 1941. - pp. 68-71
Yalkowsky S.H., Yan H., Jain P. Handbook of aqueous solubility data. – 2nd ed. - CRC Press, 2010. - pp. 20
Промышленные хлорорганические продукты: Справочник. - М.: Химия, 1978. - pp. 171-178 [Russian]
Рабинович В.А., Хавин З.Я. Краткий химический справочник. - Л.: Химия, 1977. - pp. 185, 223 [Russian]
Справочник химика. - Т. 2. - Л.-М.: Химия, 1964. - pp. 1028-1029 [Russian]
Хёрд Ч.Д. Пиролиз соединений углерода. - Л.-М.: ГОНТИ РКТП СССР, 1938. - pp. 324 [Russian]
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© Collected Ruslan Anatolievich Kiper, burewestnik@mail.ru